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Parting of the Wet-Method-Precipitates for the Assay of the M-State-Minerals These parting methods were developed in an unheated space with an ambient temperature of approximately 50 degrees Fahrenheit. Residence time adjustments may need to be made for other conditions. Various methods were tried and gave similar results but these are the easiest to reproduce for someone with limited equipment and experience. Various acids were tested, along
with buffered solutions and ammonium salts. Ultimately, the least
exotic were chosen for simplicity. While no metal is produced by these procedures, the final separation of M-Iridium from M-Gold by sublimation gives more weight loss than can be accounted for by water of hydration alone (assuming Mg(OH)2 ). This supports claims made by David Hudson and the Essene. As the separate fractions are not reduced to weighable metal, it is possible that the entire procedure is an exercise in chimerastry rather than chemistry. However, a microwave assay system does give weighable gold metal from this material, 300% above results obtainable by any standard assay procedure. This again gives some support to the claims of other researchers. These parting methods are offered
in the hope that they may be useful and perhaps even help to open
a door for discovery. I. Separation of the M-State Elements from Mg(OH)2 This method is based on several properties of Mg(OH)2. In a slurry, magnesium hydroxide has a pH of 10.5, but the pH drops to 9.0 when the slurry is being used to neutralize a mild acid. This parting must be done by hand, without mechanical agitation. Otherwise it proceeds too quickly, and M-State becomes entrained with the magnesium and lost to the filtrate. Thoroughly dried ORMUS precipitates are ground to fine powder and made into a 1.25% slurry. While stirring by hand, a 5 to 1 or weaker solution of HCl is added, a drop at a time, to bring the pH down to 8.8. Using a well-calibrated pH meter, notice how long it takes for the slurry to rebound to 9.1, while stirring vigorously. This procedure is repeated until the rebound time is more than 60 seconds. At this point, separate the solids, dry them at 275� F and regrind to fine powder. Replace the solids in the filtrate and proceed as before. When, once again, the rebound time between pH 8.8 and 9.1 becomes more than 60 seconds; filter, dry and grind the solids. Then replace them in the filtrate and proceed as before. When the rebound time between pH 8.8 and 9.1 becomes 90 seconds, or more, end point has been achieved. It is postulated that when the slurry no longer strongly exhibits its original pH characteristics, the remaining solids must be something other than Mg(OH)2. Filter and dry the solids, regrind
and weigh. II. Separation of the M-Iridium and M-Gold from the M-Rhodium and other M-State Elements. Place the ground residue from the first parting in enough water to create a 0.25% slurry. While stirring, add dilute HCl, a drop at a time to lower the pH to 5. Continue to do this until the rebound time between pH 5.4 and 6.4 is 120 seconds or more. Again, it is postulated that when the slurry no longer strongly exhibits its original pH characteristics (in this case alkalinity) parting is complete. Filter and dry the solids at 275� F, then regrind and weigh. Subtract this weight from the weight of the first parting residue. Supposing that the lost weight represents M-Rh(OH)4 or an analogue, then the lost weight x 0.602 = M-Rh. III. Separation of the M-Gold from the M-Iridium Place the residue from the second parting in an oven at 500� F for 15 minutes, to ignite carbon. Weigh the residue. Place the residue from ignition
in a retort, scorifying dish or other container capable of withstanding
sustained heat at 750� C. Weigh the residue and subtract from the original to find the lost weight. Final calculations are as follows: A. Supposing a compound M-Ir(OH)4
or an analog, which decomposes at 350� C to form M-IrO2
+ 2H2O, the weight of the residue x 0.8573
would equal the weight of M-Iridium |
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